DYNAMIC WETTING BEHAVIOR OF HEXAGONAL BORON NITRIDE BY SILVER-COPPER-TITANIUM ALLOY BRAZE AND DISSIMILAR LASER BRAZING OF HEXAGONAL BORON NITRIDE AND TUNGSTEN CARBIDE

Yoshihisa Sechi 1 Kimiaki Nagatsuka 2 Hidetoshi Fujii 3 Kazuhiro Nakata 3
1Planning Division, Kagoshima Prefectural Institute of Industrial Technology, Kirishima, Kagoshima
2Graduate school of Engineering, Osaka University, Suita, Osaka
3Joining and Welding Research Institute, Osaka University, Ibaraki, Osaka
Boron nitride ceramics have various functional characteristics. Especially, hexagonal boron nitride (h-BN) has a good thermal resistibility and solid-lubrication. Besides, as the WC-Co alloy has low thermal expansion coefficient, it is frequently applied for a counter structural material to ceramics. Meanwhile, the wettability of h-BN to the brazing metals is relatively low compared to the other ceramics [1], therefore, it is difficult to braze h-BN to another material. Thus only a fewstudies have focused on the joining of boron nitride and the tungsten carbide alloy or other metals [2].
Laser brazing has good characteristics for dissimilar joining because of possibility of a short heating time and small heating area, and suppression of damage to the base materials compared to conventional long time heating in a vacuum furnace, but the behavior of the molten alloy braze during laser brazing has not been described in detail.
In this study, the time dependence of the wettability of h-BN by Ag-Cu-Ti alloy braze was determined using a high-speed video camera, and elemental analyses of the interface were performed to describe the dissimilar laser brazing of the h-BN and WC-Co alloy, and in order to investigate the characteristics of the dissimilar joint, cross-section observations, elemental and structural analyses, and shear strength measurements were performed.
The h-BN block was set on WC-Co alloy plate. The Ag-Cu-Ti alloy braze sheet, which was based on the eutectic Ag-Cu alloy with additional Ti as an activator, was placed on the h-BN block in a chamber filled with Ar. The laser heating was carried out by selectively irradiating the WC-Co alloy plate. Just after melting of the alloy braze including 1.68mass%Ti, the droplet was not wet to the h-BN, but 2 seconds later, it started to spread, and just before the end of the heating, its contact angle was acute. Most of the Ti in the braze was consumed to form a reaction layer at the interface.
Using the same laser heating process, we made a dissimilar joint of h-BN and WC-Co. In all the shear strength tests, every crack was on the h-BN side of the interface of the brazing joint which suggested that the brazing joint interface has a sufficient strength to connect the h-BN and WC-Co.
[1] M.G. Nicholas, D.A. Mortimer, L.M. Jones, R.M. Crispin. Some observations on the wetting and bonding of nitride ceramics. J Mat Sci 1990; 25(6): 2679-89.
[2] J. Felba, K. P. Friedel, P. Krull, I.L. Pobol, H. Wohlfahrt. Electron beam activated brazing of cubic boron nitride to tungsten carbide cutting tools. Vac 2001; 62: 171-80.








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